DYES HAVE BEEN EXTENSIVELY USED IN INDUSTRIES, SUCH AS TEXTILE, PAPER, PRINTING, COSMETICS, PLASTICS AND RUBBER, FOR THE COLORATION OF PRODUCTS [1, 2]. THE DISCHARGE OF COLORED WASTE IS NOT ONLY DAMAGING THE AESTHETIC NATURE OF RECEIVING STREAMS, BUT ALSO IS TOXIC TO THE AQUATIC LIFE [2]. POLYANILINE (PAN) IS A CONDUCTING POLYMER THAT CAN BE EASILY SYNTHESIZED CHEMICALLY FROM BRONSTED ACIDIC AQUEOUS SOLUTIONS [3, 4]. THE REMOVAL DYE FROM THE WASTEWATER, BEFORE INTERRING RIVERS, IS VERY IMPORTANT. FOR TREATMENT OF THE ADSORPTION DATA, BOTH LANGMUIR AND FREUNDLICH ISOTHERM WERE EMPLOYED, THEREFORE BRILLIANT BLUE (BB) AS A TYPICAL BASIC DYE WAS SELECTED AS A TEST PROBE [4]. IN THIS RESEARCH, NANO COMPOSITE OF POLYANILINE HAZELNUT WASTE (TERMED AS PAN/HN) WAS PREPARED VIA CHEMICAL POLYMERIZATION OF ANILINE ON THE SURFACE OF HAZELNUT WASTE FOR ADSORPTION BB FROM AQUEOUS SOLUTION. THE STUDIES OF ADSORPTION WERE STUDIED BY USING LANGMUIR, FREUNDLICH EQUATIONS. THE RESULTS SHOWED THAT PAN/HN WAS A GOOD ADSORPTION FOR REMOVAL OF BRILLIANT BLUE. FINALLY, ADSORPTION OF BB ON THE SURFACE OF HAZELNUT WASTE COATED WITH PAN/HN WAS SHOWED BY USING SCANNING ELECTRON MICROSCOPY (SEM) IMAGES.